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If the DMF content versus total solids (NaOTs (sodium tosylate), NaOAc, Et 2 PMEA) is greater than 20% (by 1 H NMR) the mixture is concentrated in vacuo until distillation stops, the contents are cooled to below 40C, dichloromethane (16 kg) is added and the reactor contents at about 20 (15-25) are agitated for at least 1 hour

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