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Add the drained resin to a 1L round-bottomed flask, add the pre-configured lysis solution TFA / H 2 O / PhOMe / PhSMe (90:5:4:1, v / v) 500 mL, magnetically stirred at room temperature for 2 hours, filter the resin under reduced pressure, and collect the filtrate

Embodiment 3 [0091] Example 3: Preparation of Peptide Fragment I [0092] 44.3 g of the c-peptide resin obtained in Example 2 was weighed into a solid-phase reaction column and swollen with DMF for 30 minutes

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Erythromycin, 3-azido-3-deoxythymidine, 5-iodo-2-deoxyuridine, (+)-catechin hydrate, l-adrenaline, desloratadine, zoledronic acid monohydrate, testosterone, estriol, and oxaliplatin were purchased from Tokyo Chemical Industry Co., Ltd and used as received